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OptiMelt References www.thinkSRS.com
OptiMelt References
Measurement and Theory
1. Kenneth Nolon Carter and Kenneth N. Carter, Jr., "Meaningful Melting
Points", J. Chem. Educ. 72 (1995) 647. Note: A very careful study of MP
determinations and the proper way to observe and document results and
observations.
2. Martin Davidson, "Avoiding Errors in Melting Point Determinations",
International Labmate, vol. 23, issue 4, July 1998.
3. Gail Karet, "Make the Most of Melting Point Measurements", R&D
Magazine, July 1999, p. 61
4. Sharp, J. T., Gosney J. and Rowley A. G., "Practical Organic Chemistry, A
Student Handbook of Techniques", 1999, Chapman & Hall, NY, USA.
5. Donal Pavia, et. Al., "Introduction to Organic Laboratory Techniques: A
Microscale Appproach", 1st edition, Saunders College Publishing,
Philadelphia, USA, 1990.
6. R. L. Shriner, R. C. Fuson and D. Y. Curtin, "Systematic Identification of
Organic Compounds", 5th edition, 1966, Wiley International, NY, USA,
Chapter 4, p. 28-34.
9. W. J. Criddle, Gwynn P. Ellis, "Spectral and Chemical Characterization of
Organic Compounds: A Laboratory Handbook", 3rd edition, 1990,Wiley,
John and Sons.
7. Harding, Ken E., "Melting Point Range and Phase Diagrams- Confusing
Laboratory Textbook Descriptions", J. Chem. Educ. 76 (1999) 224.
8. Brown, R. J. C.; Brown, R. F. C., "Melting Point and Molecular Symmetry",
J. Chem. Educ. 77(2000) 724.
10. George V. D. Tiers, "Melting Points are Uncorrected"-True or False?, J.
Chem. Educ., 67 (1990) 258
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11. George V. D. Tiers, "Calibration of capillary melting point apparatus to the
International Temperature Scale of 1990 (ITS-90) by use of fluxed highly
pure metals", Analytica Chimica Acta, 237 (1990) 241
12. "OECD Guidelines for the Testing of Chemicals, Test No. 102: Melting
Point/ Melting Range", OECD Organisation for Economic Co-operation
and Development, January 2001, vol. 1, no. 1, pp. 1-8 (8 pages). Note:
The OECD Guidelines for the Testing of Chemicals are a collection of
about 100 of the most relevant internationally agreed testing methods
used by government, industry and independent laboratories to identify and
characterize potential hazards of new and existing chemical substances,
chemical preparations and chemical mixtures. Adopted in 1981, the
Guidelines have become the recognized reference tool for professionals
working on the testing of chemicals and the assessment of their potential
hazards. Purchase guidelines on-line at: http://www.sourceoecd.org/
13. Randal A. Gauthier, "Time to Learn your RTDs", Sensors, May 2003, p.
53. Note: Pt RTDs aare discussed in detail, along with some aging
guidelines.
MP Tables
1. W. Utermark, "Melting Point Tables of Organic Compounds". 2nd revised
and supplemented edition. Interscience: New York, 1963. Note: Provides
data for over 7000 compounds, arranged by increasing melting point
temperatures. While not used much today for research purposes, this
work is still valuable as a teaching tool.
2. David R. Lide, "The Handbook of Chemistry & Physics", CRC Press, 2003.
3. Patricia Heckelman, Ann Smith (Editor), Maryadele J. Oneil (Editor), "
Merck Index: An Encyclopedia of Chemicals, Drugs & Biologicals- 13th
Edition ", Merck Publishing Group , Merck &Company Inc., 2001.
Stanford Research Systems, Inc. Phone: (408) 744-9040
OptiMelt References www.thinkSRS.com
4. Amyand David Buckingham (Editor), Finlay J. MacDonald (Editor),
"Dictionary of Organic Compounds", CRC Press, 1995.
5. John A. Dean, Norbert Adolph Lange, "Lange's Handbook of Chemistry",
The McGraw-Hill Companies, 1998.
6. W. L. F. Armargo and D. D. Perrin, "Purification of Laboratory Chemicals",
4th edition, Butterworth Heinemann, Woburn, MA, USA, 1998.
7. R. L. Shriner, R. C. Fuson and D. Y. Curtin, "Systematic Identification of
Organic Compounds", 5th edition, 1966, Wiley International, NY, USA,
Chapter 4, p. 28-34.
8. "Aldrich Handbook of Fine Chemicals and Laboratory Equipment", Sigma-
Aldrich Fine Chemicals, P.O. Box 355, Milwaukee, WI 53201, USA, 2003-
2004 (www.sigma-aldrich.com.)
9. W. J. Criddle, Gwynn P. Ellis, "Spectral and Chemical Characterization of
Organic Compounds: A Laboratory Handbook", 3rd edition, 1990,Wiley,
John and Sons.
10. Zvi Rappoport (Editor), "Handbook of Tables for Organic Compound
Identification", CRC Press, 1966.
11. Farmilo, C. G. and Levi, L.: Part IA:" Introduction to identification of
narcotics by physical methods", Bulletin on Narcotics, Vol. V, No. 4. Note:
Farmilo and Levi have written several articles on the identification of
narcotics centered around melting point determinations.
12. Beilstein Files, http://info.cas.org/ONLINE/DBSS/beilstein.html. Database
provided by: MDL Information Systems GmbH, Theodor-Heuss-Allee 108,
D-60486 Frankfurt, Germany, STNmail: HLPBEILK, Phone:(+49) 69/5050-
4252, Fax:(+49) 69/5050-4245, E-mail: [email protected]. Note: this
database includes over 8 million compounds but requires subscription and
dedicated client software.
Stanford Research Systems, Inc. Phone: (408) 744-9040
OptiMelt References www.thinkSRS.com
Quality Control
GLP and GMP
1. Ludwig Huber, "Validation and Qualification in Analytical Laboratories",
Interpharm Press, Buffalo Grove, IL, USA, 1998.
2. Ludwig Huber, "A primer - Good Laboratory Practice and Current Good
Manufacturing Practice", Publication # 5968-6193E, Agilent Technologies,
Germany, March 2000.
3. Ludwig Huber, "Validation of Computerized Analytical and Networked
Systems", CRC Press, 2002.
4. Michael Anisfeld, "International Drug GMPs", Interpharm Press, Buffalo
Grove, IL, USA, August 1993.
5. Michael H. Anisfeld (Editor), " International GLPs", CRC Press, 1993.
Pharmacopoeias
1. "International Pharmacopoeia: Tests, Methods, and General
Requirements: Quality Specifications for Pharmaceutical Substances,
Excipients, and Dosage Forms", 3rd edition, volume 5, published by
WHO Staff, www.who.int (order at www.bookorders.who.int).
2. "United States Pharmacopoeia", USP 27